HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
TIBA isododecane → 2,3,5-Triiodobenzoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | TIBA isododecane | HCID 131728349 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | 2,3,5-Triiodobenzoic acid | HCID 6948 | — |
Reaktionsschritte
9.8 cc of TIBA/isododecane solution (101 g/L) were mixed with 1.91 cc of MAO/toluene solution (Albemarle -30% wt) to obtain a MAO/TIBA molar ratio of 2:1. The solution was stirred for 1 hour at room temperature. Then, 26 mg of A-1 were dissolved in the solution.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07977444B2 |
| Quelldatensatz | uspto-grants-2011_07 |
| ORD ID | ord-b1c79844f75f48d4949d31fdccf96742 |
| Quellennotiz | uspto-grants-2011_07 |