HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
trans-2-(4-Chlorophenyl)vinylboronic acid → HCID 57554998, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | trans-2-(4-Chlorophenyl)vinylboronic acid | HCID 642694 | — |
| Edukt | [1-(3-Bromo-phenyl)-3,5-dimethyl-1H-pyrazol-4-yl]-(3-diethylamino-pyrrolidin-1-yl)-methanone | HCID 67313795 | — |
| Produkt | HCID 57554998 | HCID 57554998 | 67% |
Reaktionsschritte
In analogy to the procedure described in Example 14C], [1-(3-bromo-phenyl)-3,5-dimethyl-1H-pyrazol-4-yl]-(3-diethylamino-pyrrolidin-1-yl)-methanone (Example 28A]) and trans-2-(4-chlorophenyl)vinylboronic acid gave the title compound in 67% yield as light brown foam. MS: 477.3 (MH+, 1 Cl).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07977358B2 |
| Quelldatensatz | uspto-grants-2011_07 |
| ORD ID | ord-04b8153fdbc94b5e99b877891c9a8e96 |
| Quellennotiz | uspto-grants-2011_07 |