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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1022732Erstellt: 26. Oktober 2026

Hydrochloric Acid → 2-(2-Pyridyloxy)acetic acid hydrochloride

https://huagongshe.com/reaction/1022732

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktHydrochloric AcidHCID 313—
EduktTert-butyl(pyridin-2-yloxy)acetateHCID 46168743—
LösungsmittelTetrahydrofuranHCID 8028—
Produkt2-(2-Pyridyloxy)acetic acid hydrochlorideHCID 66975989—

Reaktionsschritte

To a solution of tert-butyl(pyridin-2-yloxy)acetate (0.18 g) in THF (1.5 mL) was added 6 mol/L hydrochloric acid (1.5 mL) at 0° C., and the mixture was warmed to room temperature, and stirred for 2 hr. The solvent was evaporated under reduced pressure, and the resultant solid was recrystallized from ethyl acetate and diisopropyl ether to give the title compound (0.11 g).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08722662B2
Quelldatensatzuspto-grants-2014_05
ORD IDord-f42aa198ffd049f88bb95d785cff233c
Quellennotizuspto-grants-2014_05