HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Styrene → 1H-Pyrrole-2,5-dione, 1-phenyl-, polymer with ethenylbenzene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Styrene | HCID 7501 | — |
| Edukt | N-Phenylmaleimide | HCID 13662 | — |
| Katalysator | Azobisisobutyronitrile | HCID 6547 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | 1H-Pyrrole-2,5-dione, 1-phenyl-, polymer with ethenylbenzene | HCID 245901 | 399,6% |
Reaktionsschritte
36 g of styrene (ST), 4 g of N-phenylmaleimide (PM), 100 mg of azobisisobutyronitrile, and 50 ml of toluene were mixed, and a polymerization reaction was performed under a nitrogen atmosphere at 85° C. for 6 hours. After cooling, purification was performed by reprecipitation using chloroform-hexane. Thus, 25.6 g of an ST-PM (90:10) random copolymer (Mn=43000) was obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08735489B2 |
| Quelldatensatz | uspto-grants-2014_05 |
| ORD ID | ord-a7756f6850b0476e8ee18c48699f303d |
| Quellennotiz | uspto-grants-2014_05 |