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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1028266Erstellt: 26. Oktober 2026

Styrene → 1H-Pyrrole-2,5-dione, 1-phenyl-, polymer with ethenylbenzene

https://huagongshe.com/reaction/1028266

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktStyreneHCID 7501—
EduktN-PhenylmaleimideHCID 13662—
KatalysatorAzobisisobutyronitrileHCID 6547—
LösungsmittelTolueneHCID 1140—
Produkt1H-Pyrrole-2,5-dione, 1-phenyl-, polymer with ethenylbenzeneHCID 245901399,6%

Reaktionsschritte

36 g of styrene (ST), 4 g of N-phenylmaleimide (PM), 100 mg of azobisisobutyronitrile, and 50 ml of toluene were mixed, and a polymerization reaction was performed under a nitrogen atmosphere at 85° C. for 6 hours. After cooling, purification was performed by reprecipitation using chloroform-hexane. Thus, 25.6 g of an ST-PM (90:10) random copolymer (Mn=43000) was obtained.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08735489B2
Quelldatensatzuspto-grants-2014_05
ORD IDord-a7756f6850b0476e8ee18c48699f303d
Quellennotizuspto-grants-2014_05