HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,4-Cyclohexadiene-1,4-dicarboxylic acid, 2,5-bis(phenylamino)-, 1,4-dimethyl ester → Quinacridone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,4-Cyclohexadiene-1,4-dicarboxylic acid, 2,5-bis(phenylamino)-, 1,4-dimethyl ester | HCID 78610 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | Quinacridone | HCID 13976 | 3% |
Reaktionsschritte
A suspension of 200 g of dimethyl 2,5-dianilino-3,6-dihydroterephthalate in 1 l of water was introduced by means of a two-material nozzle and 1.5 m3 of nitrogen into a tubular reactor (50 mm in diameter, 300 mm in length) at 395° C. Using a solids filter, 170 g of dihydroquinacridone (purity 95%, includes about 3% of quinacridone) were obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04956464 |
| Quelldatensatz | uspto-grants-1990_09 |
| ORD ID | ord-1143522a44fa4207a457739f96c5b93c |
| Quellennotiz | uspto-grants-1990_09 |