2-(7-nitro-1H-indazol-4-yl)acetonitrile → 2-(3-Methoxy-4-nitrophenyl)acetonitrile

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	2-(7-nitro-1H-indazol-4-yl)acetonitrile	HCID 13629308	—
Edukt	N,N-Dimethyl-N-[2-(3-methoxy-4-nitrophenyl)ethenyl]amine	HCID 54285175	—
Produkt	2-(3-Methoxy-4-nitrophenyl)acetonitrile	HCID 13629317	99,3%

Reaktionsschritte

19.8 g of N,N-dimethyl-N-[2-(3-methoxy-4nitrophenyl)ethenyl]amine and 30.0 g of hydroxylamineorthosulfonic acid are reacted as described in connection with preparing 2-(7-nitro-1H-indazol-4-yl)acetonitrile, thus obtaining 17.0 g of (3-methoxy-4-nitrophenyl)acetonitrile, mp 85°-86.5° C.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US04958026
Quelldatensatz	uspto-grants-1990_09
ORD ID	ord-5e0df74fa9d84916b8697d0da74d71e9
Quellennotiz	uspto-grants-1990_09