Hydrochloric Acid → 1H,2H,3H-pyrrolo(3,4-c)pyridine dihydrochloride

HRID 1033747Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1033747
[CH2:1]1[C:9]2[CH:8]=[CH:7][N:6]=[CH:5][C:4]=2[CH2:3][N:2]1C(OCC)=O.[ClH:15]>>[ClH:15].[ClH:15].[CH2:1]1[C:9]2[CH:8]=[CH:7][N:6]=[CH:5][C:4]=2[CH2:3][NH:2]1

Komponenten

3

Edukt 2

HCID 313Hydrochloric AcidHCID 18953633ethyl 1H-pyrrolo[3,4-c]pyridine-2(3H)-carboxylate

Produkt 1

HCID 189536441H,2H,3H-pyrrolo(3,4-c)pyridine dihydrochloride

Versuchsvorschrift

10.4 g (51 mmol) of ethyl 2,3-dihydro-1H-pyrrolo-[3,4-c]pyridine-2-carboxylate are refluxed for 15 hours together with 100 ml of concentrated hydrochloric acid. The batch is evaporated, and the crystalline residue is stirred with acetone. The product is filtered off with suction and dried in the air.

Aufarbeitung

  1. customThe batch is evaporated
  2. filtrationThe product is filtered off with suction
  3. customdried in the air

Quellen und Nachweise

ORD-Eintrag
ord-da275ca293f44d51a9ea56983ed6266b
Quelldatensatz
uspto-grants-1994_05
Patentnummer
US05312823

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