HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1033821Erstellt: 23. Oktober 2026
3-(4-Chlorophenyl)-1-(1,1-dimethylethyl)-1H-pyrazolo(3,4-d)pyrimidin-4-amine → Lytron 810
https://huagongshe.com/de/reaction/1033821
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | 3-(4-Chlorophenyl)-1-(1,1-dimethylethyl)-1H-pyrazolo(3,4-d)pyrimidin-4-amine | HCID 4878 | — |
| Edukt | Styrene | HCID 7501 | — |
| Edukt | Maleic Anhydride | HCID 7923 | — |
| Edukt | Propylene | HCID 8252 | — |
| Edukt | (1,3-Phenylenebis(1-methylethylidene))bis(tert-butyl) peroxide | HCID 16654 | — |
| Produkt | Lytron 810 | HCID 62707 | — |
Reaktionsschritte
A thermoplastic resin composition was produced in the same manner as in Example 40, except that in place of MS-PP-2 and MS-EPM-2, a co-grafting product of the starting polypropylene for MS-PP-2 and the starting ethylene-propylene copolymer rubber for MS-EPM-2 was used. In a Hensachel mixer, 100 parts by weight of a blend of powder of the starting polypropylene for MS-PP-2 and pellets of the starting ethylene-propylene copolymer rubber for MS-EPM-2 in the ratio of 55:23 was uniformly mixed with 1.5 parts by weight of maleic anhydride, 0.5 part by weight of styrene, 0.6 part by weight of the propylene homopolymer containing as free-radical initiator 8% by weight of 1,3-bis(t-butylperoxyisopropyl)benzene (Sanperox®-TY1.3, mfd. by Sanken Kako Co., Ltd.) supported thereon, and 0.1 part by weight of 1010 (mfd. by Ciba-Geigy Ltd.) as stabilizer. The resulting mixture was melt-kneaded by means of a TEX 44 SS-30BW-2V type twin screw extruder mfd. by JAPAN STEEL WORKS, LTD., at a temperature of 220° C. for an average residence time of 1.5 minutes to obtain a (maleic anhydride-styrene)-co-grafted polypropylene/ethylene-propylene copolymer rubber having an amount of maleic anhydride added of 0.24% by weight, an amount of styrene added of 0.23% by weight and a melt flow rate of 15 g/10 min. This co-grafting product is hereinafter abbreviated as MS-(PP-2/EPM-2).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US05312867 |
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| Quelldatensatz | uspto-grants-1994_05 |
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| ORD ID | ord-6f409fa0cdae48e1bc390a7fff4ea7a7 |
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| Quellennotiz | uspto-grants-1994_05 |
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