HCID 178443886, Verbindung → HCID 178443885, Verbindung
Reaktionsgleichung
[NH2:1][C:2]1[N:6]=[C:5]([S:7][CH2:8][CH2:9][S:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])[NH:4][N:3]=1.C(SCCSCCSC1N=C2N(N=1)[C:38]([OH:41])=[CH:37][C:36]([CH3:42])=N2)CCCCC>>[CH2:11]([S:10][CH2:9][CH2:8][S:7][C:5]1[N:6]=[C:2]2[N:3]([N:4]=1)[C:38]([OH:41])=[CH:37][C:36]([CH3:42])=[N:1]2)[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]Komponenten
3
Versuchsvorschrift
Compound 14 was prepared from Compound 7 using a procedure analogous to that described previously for Compound 20. Recrystallization of the crude product from ethyl acetate gave a 59% yield of a white solid, m.p. 125.5°-127° C. Analysis: Calculated for C16H26N4OS2 : C,54.21; H, 7.39; N, 15.80. Found: C, 53.51; H, 7.21; N, 15.72.
Aufarbeitung
- customRecrystallization of the crude product from ethyl acetate
Quellen und Nachweise
- ORD-Eintrag
- ord-fcdb5380834d4d0bb01a14a4cac966ba