HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Hydrazinyl-4-iodopyridine → HCID 178453093, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Hydrazinyl-4-iodopyridine | HCID 53402897 | — |
| Edukt | Tert-butyl (1-(2-formylquinolin-8-yl)piperidin-4-yl)methylcarbamate | HCID 86654345 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | HCID 178453093 | HCID 178453093 | — |
Reaktionsschritte
To tert-butyl (1-(2-formylquinolin-8-yl)piperidin-4-yl)methylcarbamate (112 mg, 0.303 mmol) in DCM (20 mL) was added 1-(4-iodopyridin-2-yl)hydrazine (78.4 mg, 0.333 mmol). The reaction mixture was stirred for 1 hour and then taken on to directly to the next step.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08557809B2 |
| Quelldatensatz | uspto-grants-2013_10 |
| ORD ID | ord-07166c0a1907496e8a191a1a6137e0bf |
| Quellennotiz | uspto-grants-2013_10 |