HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Aluminium lithium hydride → 2-Ethoxy-4-(trifluoromethyl)benzaldehyde
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Aluminium lithium hydride | HCID 21226445 | — |
| Edukt | N-methoxy-N-methyl-2-ethoxy-4-trifluoromethyl-benzamide | HCID 86649957 | — |
| Produkt | 2-Ethoxy-4-(trifluoromethyl)benzaldehyde | HCID 22494338 | 89,1% |
Reaktionsschritte
N-Methoxy-N-methyl-2-ethoxy-4-trifluoromethyl-benzamide (1.04 g) was reacted with 1 M LAH (1 ml) at −40° C. for 2 hrs as described above to yield title compound (729 mg, 65%)
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08557872B2 |
| Quelldatensatz | uspto-grants-2013_10 |
| ORD ID | ord-c2788596af4a4dd391b226db3bbe9fb4 |
| Quellennotiz | uspto-grants-2013_10 |