HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Azide → Diisobutyl aluminium azide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Azide | HCID 33557 | — |
| Edukt | Diisobutyl aluminium chloride | HCID 16686353 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | Diisobutyl aluminium azide | HCID 86610998 | — |
Reaktionsschritte
1.235 g of granular sodium azide (19 mmol) are added to a cold solution of diisobutyl aluminium chloride (19 mmol, 1.8M in toluene) diluted in 5 ml of toluene and the mixture is stirred at room temperature over the night to give diisobutyl aluminium azide.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08569528B2 |
| Quelldatensatz | uspto-grants-2013_10 |
| ORD ID | ord-64e4130e48684bdfb9deb439bc89815c |
| Quellennotiz | uspto-grants-2013_10 |