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HRID 10484Erstellt: 23. Oktober 2026
Calcium chloride, dihydrate → Calcium bicyclo(2.2.1)heptane-2,3-dicarboxylate
https://huagongshe.com/de/reaction/10484
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Calcium chloride, dihydrate | HCID 6093260 | — |
| Edukt | bicyclo2.2.1heptane-2,3-dicarboxylic acid, disodium salt | HCID 21981355 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | Calcium bicyclo(2.2.1)heptane-2,3-dicarboxylate | HCID 21981350 | — |
Reaktionsschritte
To a solution of disodium bicyclo[2.2.1]heptane-2,3-dicarboxylate (22.6 g, 0.1 mol) in water (150 g) was added a solution of calcium chloride dihydrate (14.7 g, 0.1 mol) in water (100 g). The mixture stirred at 60° C. for 2 hours. The resulting white precipitate was filtered. The white powdery product was dried and milled (m.p. >300° C.).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US07094820B2 |
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| Quelldatensatz | uspto-grants-2006_08 |
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| ORD ID | ord-c0156d75e2c14a898911d22916c87e2d |
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| Quellennotiz | uspto-grants-2006_08 |
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