HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(2-methylphenyl)methanesulfonyl Chloride → N-[4-(2,4-Dioxo-1,2,3,4-tetrahydronaphtho[1,2-b][1,4]diazepin-5-yl)phenyl]-1-(2-methylphenyl)methanesulfonamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (2-methylphenyl)methanesulfonyl Chloride | HCID 2760661 | — |
| Edukt | 5-(4-Aminophenyl)-1H-naphtho[1,2-b][1,4]diazepine-2,4(3H,5H)-dione | HCID 117699167 | — |
| Produkt | N-[4-(2,4-Dioxo-1,2,3,4-tetrahydronaphtho[1,2-b][1,4]diazepin-5-yl)phenyl]-1-(2-methylphenyl)methanesulfonamide | HCID 117699186 | 37% |
Reaktionsschritte
By using 5-(4-aminophenyl)-1H-naphtho[1,2-b][1,4]diazepine-2,4(3H,5H)-dione obtained in Example 1, (3), and o-tolyl-methanesulfonyl chloride, the title compound (yield 37%) was obtained in the same manner as that of Example 145.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09382236B2 |
| Quelldatensatz | uspto-grants-2016_07 |
| ORD ID | ord-c2e876baa7524b1ea6d127aa961fdbf4 |
| Quellennotiz | uspto-grants-2016_07 |