HCID 83702359, Verbindung → HCID 89699660, Verbindung
Reaktionsgleichung
[CH3:1][C:2]1[CH:8]=[CH:7][C:5]([NH2:6])=[CH:4][C:3]=1[N:9]1[C:16]2[N:12]([N:13]=[C:14]([C:17]3[CH:18]=[N:19][CH:20]=[CH:21][CH:22]=3)[CH:15]=2)[CH:11]=[CH:10]1.[C:23]([C:27]1[CH:28]=[C:29]([CH:33]=[C:34]([NH:36][CH3:37])[N:35]=1)[C:30](O)=[O:31])([CH3:26])([CH3:25])[CH3:24]>>[C:23]([C:27]1[CH:28]=[C:29]([CH:33]=[C:34]([NH:36][CH3:37])[N:35]=1)[C:30]([NH:6][C:5]1[CH:7]=[CH:8][C:2]([CH3:1])=[C:3]([N:9]2[C:16]3[N:12]([N:13]=[C:14]([C:17]4[CH:18]=[N:19][CH:20]=[CH:21][CH:22]=4)[CH:15]=3)[CH:11]=[CH:10]2)[CH:4]=1)=[O:31])([CH3:26])([CH3:24])[CH3:25]Komponenten
3
Versuchsvorschrift
60 mg (0.21 mmol) of the compound of Example 6A and 43 mg (0.21 mmol) of the compound of Example 44A were reacted analogously to the procedure of Example 33, except that in this case the reaction time was 16 h. This gave 31 mg (31% of theory) of the title compound.
Quellen und Nachweise
- ORD-Eintrag
- ord-c5928560833f44658e84f44c806a5b1d
- Quelldatensatz
- uspto-grants-2016_07
- Patentnummer
- US09394309B2
Notizen zur Reaktion
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