HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Pivalic acid → n-Neopentanoyl-2-butyloctylamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Pivalic acid | HCID 6417 | — |
| Edukt | 2-Butyl-n-octan-1-amine | HCID 18673284 | — |
| Lösungsmittel | Heptane | HCID 8900 | — |
| Produkt | n-Neopentanoyl-2-butyloctylamine | HCID 18673286 | 76% |
Reaktionsschritte
10.4 g of pivalic acid and 17.2 g of 2-butyloctylamine were mixed together in the tube of a microwave machine (Maxidigest™ MX 350 from the company Prolabo; frequency 2450±50 MHz, modulable power 300 W). After irradiation for about 1 hour at 160° C.±10° C., the reaction mixture was dissolved in heptane and then purified on silica. 19 g of the desired amide were obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06515178B2 |
| Quelldatensatz | uspto-grants-2003_02 |
| ORD ID | ord-0f0a5b5bf37040aa887e212132840b2f |
| Quellennotiz | uspto-grants-2003_02 |