Benzyl chloroformate → HCID 178465414, Verbindung
Reaktionsgleichung
[NH2:1][CH:2]([PH:4](=[O:6])[OH:5])[CH3:3].Cl[C:8]([O:10][CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)=[O:9]>>[C:12]1([CH2:11][O:10][C:8]([NH:1][CH:2]([PH:4](=[O:5])[OH:6])[CH3:3])=[O:9])[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1Komponenten
3
Versuchsvorschrift
The process is performed according to the operating conditions described in 1.4., starting with 1.7 g (15.6 mmol) of (1-aminoethyl)phosphinic acid and 3.12 g (18.29 mmol) of benzyl chloroformate. 2.8 g of product are recovered (yeld=73.9%).
Aufarbeitung
- custom2.8 g of product are recovered (yeld=73.9%)
Quellen und Nachweise
- ORD-Eintrag
- ord-d591f6ba6a6c43e6a4e593f2c2df6e51
- Quelldatensatz
- uspto-grants-2003_02
- Patentnummer
- US06518260B1
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