2-Chlorooxane → N-(2-tetrahydropyranyloxy)-tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-amine
Reaktionsgleichung
[CH2:1]([O:4][N:5]([C:16]([CH3:19])([CH3:18])[CH3:17])[C:6]([CH3:15])([CH3:14])[C:7]([NH:9][C:10]([CH3:13])([CH3:12])[CH3:11])=[O:8])[CH:2]=[CH2:3].C(N([C:26](C)(C)[C:27](NC(C)(C)C)=[O:28])O)(C)(C)C.ClC1CCCCO1>>[O:28]1[CH2:27][CH2:26][CH2:3][CH2:2][CH:1]1[O:4][N:5]([C:16]([CH3:19])([CH3:18])[CH3:17])[C:6]([CH3:15])([CH3:14])[C:7]([NH:9][C:10]([CH3:13])([CH3:12])[CH3:11])=[O:8]Komponenten
4
Edukt 3
Produkt 1
Versuchsvorschrift
The compound is prepared in analogy to compound (204) from tert-butyl-(dimethyl-tert-butylaminocarbonyl-methyl)-hydroxylamine and 2-chlor-tetrahydropyrane in 33% yield as colorless oil.