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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1059706Erstellt: 26. Oktober 2026

(5-(1-Hydroxy-1-methyl-ethyl))-pyridine-2-sulfonic acid amide → 2-Pyridinesulfonamide, 5-(1-methylethenyl)-

https://huagongshe.com/reaction/1059706

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt(5-(1-Hydroxy-1-methyl-ethyl))-pyridine-2-sulfonic acid amideHCID 54360667—
LösungsmittelTrifluoroacetic acidHCID 6422—
Produkt2-Pyridinesulfonamide, 5-(1-methylethenyl)-HCID 45080641—

Reaktionsschritte

A solution of 0.1 g of (5-(1-hydroxy-1-methyl-ethyl))-pyridine-2-sulfonic acid amide in CF3CO2H (2 ml) was refluxed for 20 h. The solvent was then removed in vacuo to give 5-isopropenyl-pyridine-2-sulfonic acid amide as a white solid which was essentially pure. El mass spectrum, m/e 198 (M calculated for C8H10N2O2S: 198).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06521631B2
Quelldatensatzuspto-grants-2003_02
ORD IDord-8e47057e93b544cfb904eb7f51a2b3b8
Quellennotizuspto-grants-2003_02