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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 10607Erstellt: 23. Oktober 2026

Pyridine → 2-(2',6'-Diisopropylphenylazo)-4-methyl-6-(9-anthracenyl)phenol

https://huagongshe.com/de/reaction/10607

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPyridineHCID 1049—
EduktSodium HydroxideHCID 14798—
EduktDiisopropylanilineHCID 32484—
EduktPhenolateHCID 119047—
Edukt2-(9-Anthracenyl)-4-methylphenolHCID 21981551—
LösungsmittelBenzeneHCID 241—
LösungsmittelWaterHCID 962—
Produkt2-(2',6'-Diisopropylphenylazo)-4-methyl-6-(9-anthracenyl)phenolHCID 136104165—

Reaktionsschritte

This phenol was prepared, as described above, from a theoretical yield of 3.9 mmol of diazotized 2,6-diisopropylaniline and a phenolate solution comprised of 2-(9-Anthracenyl)-4-methylphenol (0.63 g), water (20 mL), NaOH (20 mmol), pyridine (2 mL), and benzene (4 mL). In this case, the product was eluted with ether:hexanes (1:10). Yield=0.30 g (29%).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07094848B2
Quelldatensatzuspto-grants-2006_08
ORD IDord-966493f923fe4472bb4fc0c0429b9e71
Quellennotizuspto-grants-2006_08