HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,2-Dodecanediol → 2-Decyl-2,3-dihydrothieno[3,4-b][1,4]dioxine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,2-Dodecanediol | HCID 92866 | — |
| Edukt | 3,4-Dimethoxythiophene | HCID 3613501 | — |
| Produkt | 2-Decyl-2,3-dihydrothieno[3,4-b][1,4]dioxine | HCID 9856993 | — |
Reaktionsschritte
Racemic 2-n-decyl-2,3-dihydro-thieno[3,4-b][1,4]dioxine was synthesized by transetherification of 3,4-dimethoxythiophene with racemic 1,2-dodecanediol as described in EXAMPLE 1. It was characterized by GC-MS and H-NMR-spectroscopy, and exhibited no optical rotation.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07094865B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-ea20d853f7c44473a5eaaef5b2e39442 |
| Quellennotiz | uspto-grants-2006_08 |