HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dimethylformamide → 1-Chloro-5-methoxy-4-methyl-2-nitrobenzene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dimethylformamide | HCID 6228 | — |
| Edukt | 4-Chloro-2-fluoro-5-nitrotoluene | HCID 87593 | — |
| Produkt | 1-Chloro-5-methoxy-4-methyl-2-nitrobenzene | HCID 21671107 | — |
Reaktionsschritte
A solution of 2-chloro-4-floro-5-methylnitrobenzene (1 mmole) in DMF (5 mL) was treated with fresh sodium methoxy (1.1 mmole), and the mixture was stirred for 6 h. Evaporation and chromatography gave 2-chloro-4-methoxy-5-methylnitrobenzene.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06965033B2 |
| Quelldatensatz | uspto-grants-2005_11 |
| ORD ID | ord-23287deedc514f49b56bdf8455dd4c18 |
| Quellennotiz | uspto-grants-2005_11 |