HCID 22280189, Verbindung → 2,5-Dimethyl-4-thiocyanato-phenol
Reaktionsgleichung
COC1C(SC#N)=CC(C)=C(O)C=1.COC(=O)C[O:18][C:19]1[CH:24]=[C:23]([CH3:25])[C:22]([S:26][C:27]#[N:28])=[CH:21][C:20]=1[CH3:29]>>[CH3:29][C:20]1[CH:21]=[C:22]([S:26][C:27]#[N:28])[C:23]([CH3:25])=[CH:24][C:19]=1[OH:18]Komponenten
3
Versuchsvorschrift
The title compound was prepared in a manner analogous to compound 1B. 400 MHz 1H NMR (DMSO-d6) δ 10.0 (s, 1H), 7.35 (s, 1H), 6.73 (s, 1H), 2.3 (s, 3H), 2.04 (s, 3H); MS m/z 180 (m+1). Preparation of (2,5-Dimethyl-4-thiocyanato-phenoxy)-acetic acid methyl ester (Compound WWB)
Quellen und Nachweise
- ORD-Eintrag
- ord-25031e1a76204c62ade45b72b495a53f
- Quelldatensatz
- uspto-grants-2005_11
- Patentnummer
- US06964983B2
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