Acetyl chloride → 2-Acetamidodibenzothiophene

HRID 1064016

Reaktionsgleichung

[NH2:1][C:2]1[CH:14]=[CH:13][C:5]2[S:6][C:7]3[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=3[C:4]=2[CH:3]=1.[C:15](Cl)(=[O:17])[CH3:16]>>[C:15]([NH:1][C:2]1[CH:14]=[CH:13][C:5]2[S:6][C:7]3[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=3[C:4]=2[CH:3]=1)(=[O:17])[CH3:16]

Komponenten

Edukt 2

HCID 6367Acetyl chloride

HCID 2984422-Dibenzothiophenamine

Produkt 1

HCID 1086272-Acetamidodibenzothiophene

Versuchsvorschrift

The title compound was prepared following the procedure of Example 2 using 2-aminodibenzthiophene (Bull. Soc. Chim. Fr. (1996), 133(6), 597-610) and acetyl chloride. NMR: 10.13 (brs, 1H), 8.6 (d, 1H), 8.15 (m, 1H), 8.0 (m, 1H), 7.9 (d, 1H), 7.6 (dd, 1H), 7.5 (m, 2H), 2.1 (s, 3H); m/z 242.

Quellen und Nachweise

ORD-Eintrag: ord-97d46ed1c2b1486398122dc0192ba12d
Quelldatensatz: uspto-grants-2005_11
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US06967216B2

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