Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Water | HCID 962 | — |
| Edukt | Lead monoxide | HCID 14827 | — |
| Edukt | Ammonium Oleate | HCID 6435897 | — |
| Lösungsmittel | Acetic Acid | HCID 176 | — |
| Produkt | Lead stearate | HCID 61258 | — |
Reaktionsschritte
Separately, 3.5 l of warm water maintained at 70° C. was charged in a stainless steel beaker having a capacity of 10 l, and 419 g of stearic acid was added and dissolved under heating. Then, 24.0 cc of 7 N aqueous ammonia was dropped to the solution and the mixture was stirred and homogeneously emulsified to form an ammonia soap liquid. Separately, 725 cc of a lead monoxide slurry (PbO-DS) having a concentration of 680 g/l, 1 l of water and 14.2 cc of acetic acid having a concentration of 2.7 moles/liter were charged in a high-speed stirrer-equipped stainless steel vessel having a capacity of 10 l, and the mixture was maintained at 70° C. The above-mentioned ammonia soap liquid was added to this lead monoxide slurry and reaction was carried out under agitation to form a lead stearate slurry.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US04329182 |
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| Quelldatensatz | uspto-grants-1982_05 |
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| ORD ID | ord-72d1730077364948b7eb6e358c9b16df |
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| Quellennotiz | uspto-grants-1982_05 |
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