HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Hydroxide → Methyl 2-benzylidene-3-hydroxypropionate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | Methyl 2-[(acetyloxy)methyl]-3-phenylprop-2-enoate | HCID 53678280 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | Methyl 2-benzylidene-3-hydroxypropionate | HCID 54265908 | — |
Reaktionsschritte
The crude product (2.1917 g) of methyl 2-benzylidene-3-acetoxypropionate obtained in Example 13 was dissolved in 15 ml of methanol, and 84 mg (97%, 2.04 mmols) of sodium hydroxide were added thereto. The mixture was stirred at room temperature for 4 hours to form methyl 2-benzylidene-3-hydroxypropionate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06242635B1 |
| Quelldatensatz | uspto-grants-2001_06 |
| ORD ID | ord-c62619cd183b43d4b504d2fff2143bda |
| Quellennotiz | uspto-grants-2001_06 |