Allyl bromide → HCID 22397836, Verbindung

Reaktionsgleichung

[CH3:1][S:2]([C:5]1[CH:6]=[C:7]([CH:11]2[CH2:16][CH2:15][NH:14][CH2:13][CH2:12]2)[CH:8]=[CH:9][CH:10]=1)(=[O:4])=[O:3].[CH2:17](Br)[CH:18]=[CH2:19]>>[CH2:19]([N:14]1[CH2:15][CH2:16][CH:11]([C:7]2[CH:8]=[CH:9][CH:10]=[C:5]([S:2]([CH3:1])(=[O:4])=[O:3])[CH:6]=2)[CH2:12][CH2:13]1)[CH:18]=[CH2:17]

Komponenten

Edukt 2

HCID 7841Allyl bromide

HCID 129889574-(3-(Methylsulfonyl)phenyl)piperidine

Produkt 1

HCID 22397836HCID 22397836, Verbindung

Versuchsvorschrift

Beginning with 4-(3-methanesulfonyl-phenyl)-piperidine and allylbromide, the titled compound was recovered by the procedure described in Example 1. MS m/z (relative intensity, 70 eV) 279 (M+, 74), 96 (bp), 82 (98), 68 (74), 55 (93). Rf=0.42 (MeOH, 0.08 (EtOAc).

Aufarbeitung

customthe titled compound was recovered by the procedure

Quellen und Nachweise

ORD-Eintrag: ord-83a5f06d83e8433598363db5c4cf32e7
Quelldatensatz: uspto-grants-2005_06
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US06903120B2

Notizen zur Reaktion

Wird geladen…