Hydrogen Peroxide → Bis(perfluoropentanoyl) peroxide

HRID 1072954

Reaktionsgleichung

Reaktionsgleichung von HRID 1072954
[OH:1][OH:2].FC(F)(F)C(F)(F)C(F)(F)C(F)(F)C([O:10][C:11](=O)[C:12]([F:24])([F:23])[C:13]([F:22])([F:21])[C:14]([F:20])([F:19])[C:15]([F:18])([F:17])[F:16])=O>FC(F)(F)C(F)(F)C(F)(F)C(F)(F)C(O)=O>[F:19][C:14]([F:20])([C:15]([F:16])([F:17])[F:18])[C:13]([F:21])([F:22])[C:12]([F:24])([F:23])[C:11]([O:1][O:2][C:11](=[O:10])[C:12]([F:23])([F:24])[C:13]([F:21])([F:22])[C:14]([F:19])([F:20])[C:15]([F:18])([F:17])[F:16])=[O:10]

Komponenten

4

Edukt 2

HCID 784Hydrogen PeroxideHCID 2769668Perfluoropentanoic anhydride

Produkt 1

HCID 11307027Bis(perfluoropentanoyl) peroxide

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 75921Perfluoropentanoic acidLösungsmittel

Versuchsvorschrift

In a manner similar to that of Example 1, H2O2 (>95%) was combined with nonafluorovaleric anhydride to give bis(nonafluoropentanoyl) peroxide (δ−83.2, −117.9, −124.8, −127.5) in nonafluorovaleric acid.

Quellen und Nachweise

ORD-Eintrag
ord-65eb4b8ace61485090d29fa6e853623b
Quelldatensatz
uspto-grants-2005_06
Patentnummer
US06911561B2

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