Hydrochloric Acid → HCID 22155954, Verbindung

HRID 1074199Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1074199
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10][C:11]2[NH:12][CH:13]=[CH:14][N:15]=2)=[CH:6][CH:5]=1)([O-:3])=[O:2].[ClH:16]>CO.C(O)C>[ClH:16].[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10][C:11]2[NH:15][CH:14]=[CH:13][N:12]=2)=[CH:6][CH:5]=1)([O-:3])=[O:2]

Komponenten

5

Edukt 2

HCID 313Hydrochloric AcidHCID 150774982-[(4-Nitrophenyl)thio]-1H-imidazole

Produkt 1

HCID 22155954HCID 22155954, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 2

HCID 702EthanolLösungsmittelHCID 887MethanolLösungsmittel

Versuchsvorschrift

The product from Example 26 was dissolved in methanol and treated with an excess of hydrogen chloride in ethyl alcohol. The mixture was concentrated and the residue triturated with ether and filtered. The solid was recrystallized from methanol to give the product as colorless prisms, mp 235°-240° C. (sealed tube).

Aufarbeitung

  1. concentrationThe mixture was concentrated
  2. customthe residue triturated with ether
  3. filtrationfiltered
  4. customThe solid was recrystallized from methanol
  5. customto give

Quellen und Nachweise

ORD-Eintrag
ord-02409625d3164c6985dedd1c1d7c52dc
Quelldatensatz
uspto-grants-1990_11
Patentnummer
US04973599

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