HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzyl Chloride → Benzyl 4-Hydroxybenzoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzyl Chloride | HCID 7503 | — |
| Edukt | Sodium 4-hydroxybenzoate | HCID 16219477 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | Benzyl 4-Hydroxybenzoate | HCID 7180 | 74% |
Reaktionsschritte
Sodium p-hydroxybenzoate (64 g) and 51 g of benzyl chloride were added to 150 g of dimethylformamide, and reacted at 100° C. for 3 hours. Benzyl p-hydroxybenzoate was obtained in a yield of 74%. The ratio of benzyl p-benzyloxybenzoate, a by-product, formed was 10%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04973737 |
| Quelldatensatz | uspto-grants-1990_11 |
| ORD ID | ord-8ad97fb84fbe49b499868575a5da03c6 |
| Quellennotiz | uspto-grants-1990_11 |