Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | 1-Bromo-3-chloropropane | HCID 8006 | — |
| Edukt | N,N-Dimethylhexylamine | HCID 78090 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | HCID 85711135 | HCID 85711135 | — |
Reaktionsschritte
A 500 mL, 3-necked, round-bottomed flask equipped with air condensers and a magnetic stirring plate was charged with N,N-dimethylhexylamine (199.46 grams, 1.54 moles), 1-bromo-3-chloropropane (243.00 grams, 1.54 moles) and 250 mL of methanol The reaction was maintained at 65° C. for 24 hours. Solvent was removed by rotary evaporation under reduced pressure to yield a brown, viscous oil. Yield 445.8 grams (1.55 moles, 100%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US05900475 |
|---|
| Quelldatensatz | uspto-grants-1999_05 |
|---|
| ORD ID | ord-baddc76a16574c178672bdf5acd2d27b |
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| Quellennotiz | uspto-grants-1999_05 |
|---|
