HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Toluenesulfonyl chloride → N-Benzyl-3,4-dimethoxyamphetamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Edukt | Benzylamine | HCID 7504 | — |
| Edukt | 3,4-Dimethoxy-alpha-methylbenzeneethanol | HCID 89187 | — |
| Produkt | N-Benzyl-3,4-dimethoxyamphetamine | HCID 410200 | — |
Reaktionsschritte
The 1-(3,4-dimethoxyphenyl)-2-propanol obtained above was subjected to sulfonylation by p-toluenesulfonyl chloride and reacted with benzylamine to give N-benzyl-3,4-dimethoxyamphetamine. The resultant compound was converted into 3,4-dimethoxyamphetamine by hydrogenation decomposition under hydrogen atmosphere with 5% Pd-C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05902900 |
| Quelldatensatz | uspto-grants-1999_05 |
| ORD ID | ord-028b640de99046ed98364198a9c82c25 |
| Quellennotiz | uspto-grants-1999_05 |