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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1075819Erstellt: 26. Oktober 2026

Water → N-methyl-2H-3-isoquinolone

https://huagongshe.com/reaction/1075819

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktWaterHCID 962—
EduktSodium BicarbonateHCID 516892—
EduktN-methyl-2H-3-isoquinolone sulfateHCID 21541268—
LösungsmittelChloroformHCID 6212—
ProduktN-methyl-2H-3-isoquinoloneHCID 12435498—

Reaktionsschritte

70 g. N-methyl-2H-3-isoquinolone sulfate are dissolved, under an atmosphere of nitrogen, in 900 ml. water. 75 g. sodium bicarbonate are added and the mixture is stirred with 500 ml. chloroform. By decantation, there is obtained a chloroform solution of N-methyl-2H-3-isoquinolone, which can be dried over anhydrous sodium sulfate and employed as such or concentrated for a further reaction.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS03954771
Quelldatensatzuspto-grants-1976_05
ORD IDord-c078a18486cf4a12876c27b719da7b99
Quellennotizuspto-grants-1976_05