HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Formaldehyde → N-methylpropylurea (morpholinomethyl)propylurea
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Formaldehyde | HCID 712 | — |
| Edukt | Morpholine | HCID 8083 | — |
| Edukt | Urea, 1,1-dipropyl-3-methyl- | HCID 215877 | — |
| Produkt | N-methylpropylurea (morpholinomethyl)propylurea | HCID 86733424 | — |
Reaktionsschritte
1 mol of N-methyl dipropylurea and 1 mol of formol in aqueous 30% solution are mixed. To this solution 1 mol of morpholine is slowly added while cooling. The stirring is maintained one hour after the end of the N-methyl dipropylurea addition. After evaporation to dryness a crystalline product is obtained which melts at 110°C. The yield of the reaction is 98%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US03957774 |
| Quelldatensatz | uspto-grants-1976_05 |
| ORD ID | ord-6cd7fcff60ed43e0b748a5001dd441f9 |
| Quellennotiz | uspto-grants-1976_05 |