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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1076997Erstellt: 26. Oktober 2026

Formaldehyde → HCID 21535614, Verbindung

https://huagongshe.com/reaction/1076997

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktFormaldehydeHCID 712—
EduktNaphthalimideHCID 66491—
Edukt4-(N-Propionylaniline)piperidineHCID 259381—
LösungsmittelDimethylformamideHCID 6228—
ProduktHCID 21535614HCID 21535614—

Reaktionsschritte

An equimolar mixture of 4-(N-propionylanilino)piperidine, aqueous formaldehyde, and 1,8-naphthalimide is suspended in a small amount of dimethylformamide and the mixture is heated until dissolution is complete. The solution is allowed to stand at room temperature and the resulting precipitate is filtered off and dried to yield N-[1-[(1,3-dihydro-1,3-dioxo-2H-benz[de]isoquinolin-2-yl)methyl]-4-piperidinyl]-N-phenylpropanamide.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS03959286
Quelldatensatzuspto-grants-1976_05
ORD IDord-fd5645c8b7274977960199a92827b267
Quellennotizuspto-grants-1976_05