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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1077480Erstellt: 26. Oktober 2026

3-(2,4-Dimethoxyphenyl)prop-2-enoic acid → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(2,4-dimethoxyphenyl)ethenyl)-, (E)-

https://huagongshe.com/reaction/1077480

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt3-(2,4-Dimethoxyphenyl)prop-2-enoic acidHCID 85636—
Edukt5,6-Diamino-1,3-diethyluracilHCID 4572133—
Produkt1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(2,4-dimethoxyphenyl)ethenyl)-, (E)-HCID 644885320%

Reaktionsschritte

Substantially the same procedure as in Reference Example 70 was repeated using 2.50 g (12.6 mmol) of 5,6-diamino-1,3-diethyluracil and 2.89 g (13.9 mmol) of 2,4-dimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from dimethylformamide/ethanol to give 0.92 g (yield 20%) of Compound 77 as yellow crystals.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05543415
Quelldatensatzuspto-grants-1996_08
ORD IDord-569161679ccf42b094902e8b5168cb09
Quellennotizuspto-grants-1996_08