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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1077491Erstellt: 26. Oktober 2026

5,6-Diamino-1,3-dimethyluracil → 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(2,4-dimethoxyphenyl)ethenyl)-1,3-dimethyl-, (E)-

https://huagongshe.com/reaction/1077491

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt5,6-Diamino-1,3-dimethyluracilHCID 79501—
Edukt3-(2,4-Dimethoxyphenyl)prop-2-enoic acidHCID 85636—
Produkt1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(2,4-dimethoxyphenyl)ethenyl)-1,3-dimethyl-, (E)-HCID 644886811%

Reaktionsschritte

Substantially the same procedure as in Reference Example 70 was repeated using 1.0 g (5.88 mmol) of 5,6-diamino-1,3-dimethyluracil and 1.35 g (6.48 mmol) of 2,4-dimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from dimethylformamide to give 221 mg (yield 11%) of Compound 99 as pale yellow grains.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05543415
Quelldatensatzuspto-grants-1996_08
ORD IDord-8c3992dd03e94feea4b42622d098c4ba
Quellennotizuspto-grants-1996_08