HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1080665Erstellt: 26. Oktober 2026
Triethylamine → N-methoxyacetyl-2-(3,4-dichlorophenyl)-4-(tetrahydropyran-2-yloxy)butylamin
https://huagongshe.com/reaction/1080665
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Triethylamine | HCID 8471 | — |
| Edukt | Methoxyacetic Acid | HCID 12251 | — |
| Edukt | Benzotriazol-1-yloxy-tris(dimethylamino)phosphonium hexafluorophosphate | HCID 151348 | — |
| Edukt | 2-(3-(3,4-Dichlorophenyl)-4-aminobutyl)oxytetrahydropyran | HCID 15670808 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | N-methoxyacetyl-2-(3,4-dichlorophenyl)-4-(tetrahydropyran-2-yloxy)butylamin | HCID 19705334 | — |
Reaktionsschritte
A mixture of 8.6 g of 2-(3,4-dichlorophenyl)-4-(tetrahydropyran-2-yloxy)butylamine (obtained according to PREPARATION (I), step (b)), 2.46 g of methoxyacetic acid, 5.55 g of triethylamine in 50 ml of dichloromethane is cooled to 0° C. and 14.5 g of BOP is added thereto.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US05583134 |
|---|
| Quelldatensatz | uspto-grants-1996_12 |
|---|
| ORD ID | ord-d869a7a1c87b484e90982da20f43cc84 |
|---|
| Quellennotiz | uspto-grants-1996_12 |
|---|
