1-Propene-1,1,3-tricarbonitrile, 2-phenyl- → 3-[[4-(Diethylamino)phenyl]imino]-2-phenyl-1-propene-1,1,3-tricarbonitrile
Reaktionsgleichung
[C:1]1([C:7]([CH2:13][C:14]#[N:15])=[C:8]([C:11]#[N:12])[C:9]#[N:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:16]([N:20]([CH2:29][CH2:30]CC)[C:21]1[CH:26]=[CH:25][C:24]([N:27]=O)=[CH:23][CH:22]=1)[CH2:17]CC>>[CH2:29]([N:20]([CH2:16][CH3:17])[C:21]1[CH:26]=[CH:25][C:24]([N:27]=[C:13]([C:14]#[N:15])[C:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)=[C:8]([C:11]#[N:12])[C:9]#[N:10])=[CH:23][CH:22]=1)[CH3:30]Komponenten
3
Versuchsvorschrift
The above procedure was used for the preparation of 3-[[4-dibutylamino)phenyl]imino]-2-phenyl-1-propene-1,1,3-tricarbonitrile using N,N-dibutyl-4-nitrosoaniline in place of N,N-diethyl-4-nitrosoaniline.
Quellen und Nachweise
- ORD-Eintrag
- ord-38924de5781742998f161ae7a2808fa7
- Quelldatensatz
- uspto-grants-1996_12