3-(3,5-Diiodo-4-hydroxybenzoyl)-2-methyl-benzofuran → KB-130015
Reaktionsgleichung
CC1OC2C=CC=CC=2C=1C(=O)C1C=C(I)C(O)=C(I)C=1.[CH2:22]([C:26]1[O:27][C:28]2[CH:49]=[CH:48][CH:47]=[CH:46][C:29]=2[C:30]=1[C:31](=O)[C:32]1[CH:37]=[C:36]([I:38])[C:35]([O:39][CH2:40][C:41]([OH:43])=[O:42])=[C:34]([I:44])[CH:33]=1)CCC>>[CH3:22][C:26]1[O:27][C:28]2[CH:49]=[CH:48][CH:47]=[CH:46][C:29]=2[C:30]=1[CH2:31][C:32]1[CH:37]=[C:36]([I:38])[C:35]([O:39][CH2:40][C:41]([OH:43])=[O:42])=[C:34]([I:44])[CH:33]=1Komponenten
3
Versuchsvorschrift
Steps 3 and 4 are performed in analogy with the steps 2 and 3 of the synthesis of (011) Step 5 is performed in analogy with the step 4 of the synthesis of (005).
Quellen und Nachweise
- ORD-Eintrag
- ord-94513a37b0e5449dbeb3e8987d6f9a3e
- Quelldatensatz
- uspto-grants-1996_12