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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1081855Erstellt: 26. Oktober 2026

3',4'-Dimethoxycinnamic acid → 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(3,4-dimethoxyphenyl)ethenyl)-1,3-di-2-propenyl-, (E)-

https://huagongshe.com/reaction/1081855

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt3',4'-Dimethoxycinnamic acidHCID 16848—
Edukt1,3-Diallyl-5,6-diaminouracilHCID 13525062—
Produkt1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(3,4-dimethoxyphenyl)ethenyl)-1,3-di-2-propenyl-, (E)-HCID 644897254,2%

Reaktionsschritte

Substantially the same procedure as in Reference Example 1 was repeated using 2.9 g (13.1 mmol) of 1,3-diallyl-5,6-diaminouracil and 2.99 g (14.4 mmol) of 3,4-dimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane/water to give 2.80 g (yield 54%) of Compound 190 as pale yellow flocculent precipitates.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05587378
Quelldatensatzuspto-grants-1996_12
ORD IDord-414349ad2ed3460e8ca1e0bede9427d4
Quellennotizuspto-grants-1996_12