HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Chlorophthalic anhydride → Methyl 3-(5-chloro-1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-(2-methyl-[1,3]dioxolan-2-yl)propionate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Chlorophthalic anhydride | HCID 67044 | — |
| Edukt | Methyl 3-amino-2-(2-methyl-[1,3]dioxolan-2-yl)propionate | HCID 21982209 | — |
| Produkt | Methyl 3-(5-chloro-1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-(2-methyl-[1,3]dioxolan-2-yl)propionate | HCID 21982220 | — |
Reaktionsschritte
Methyl 3-(5-chloro-1,3-dioxo-1,3-dihydro-isoindol-2-yl)-2-(2-methyl-[1,3]dioxolan-2-yl)propionate was prepared (0.54 g, 73%) in the same manner as described in the above example 5 (1) from methyl 3-amino-2-(2-methyl-[1,3]dioxolan-2-yl)propionate (0.40 g, 2.11 mmol) and 4-chlorophthalic anhydride (0.50 g, 2.74 mmol), and the obtained product was identified with the following NMR data.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07094908B2 |
| Quelldatensatz | uspto-grants-2006_08 |
| ORD ID | ord-ba36ac71896c4e299590b9da60b729a0 |
| Quellennotiz | uspto-grants-2006_08 |