Reaktionsgleichung
[NH2:1][CH2:2][CH:3]([C:8]1([CH3:13])[O:12][CH2:11][CH2:10][O:9]1)[C:4]([O:6][CH3:7])=[O:5].[CH:14]1[CH:19]=[C:18]2[CH:20]=[CH:21][C:22]3[C:27](=O)[O:26][C:24](=[O:25])[C:23]=3[C:17]2=[CH:16][CH:15]=1>>[O:25]=[C:24]1[C:23]2[C:17]3[CH:16]=[CH:15][CH:14]=[CH:19][C:18]=3[CH:20]=[CH:21][C:22]=2[C:27](=[O:26])[N:1]1[CH2:2][CH:3]([C:8]1([CH3:13])[O:9][CH2:10][CH2:11][O:12]1)[C:4]([O:6][CH3:7])=[O:5]Komponenten
3
Versuchsvorschrift
Methyl 3-(1,3-dioxo-1,3-dihydro-benzo[e]isoindol-2-yl)-2-(2-methyl-[1,3]dioxolan-2-yl)propionate was prepared (0.45 g, 58%) in the same manner as described in the above example 5 (1) from methyl 3-amino-2-(2-methyl-[1,3]dioxolan-2-yl)propionate (0.40 g, 2.11 mmol) and 1,2-naphthalic anhydride (0.55 g, 2.75 mmol), and the obtained product was identified with the following NMR data.
Quellen und Nachweise
- ORD-Eintrag
- ord-507b77cf8a6148b682e37f9d01ce208c
- Quelldatensatz
- uspto-grants-2006_08
- Patentnummer
- US07094908B2
Verknüpfte Notizen
Wird geladen…