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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1085964Erstellt: 26. Oktober 2026

4-Acetylpyridine → Cyclohexanecarboxylic acid [1-(4-pyridinyl)ethylidene]hydrazide

https://huagongshe.com/reaction/1085964

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt4-AcetylpyridineHCID 14282—
EduktCyclohexanecarbohydrazideHCID 240039—
LösungsmittelEthanolHCID 702—
ProduktCyclohexanecarboxylic acid [1-(4-pyridinyl)ethylidene]hydrazideHCID 333758173,1%

Reaktionsschritte

A solution of 4.26 gm (0.03 mole) of cyclohexanecarboxylic acid hydrazide, 3.63 gm (0.03 mole) of 4-acetylpyridine and 100 ml of ethanol is refluxed 7 hr. The solvent is evaporated in vacuo to give a white solid. The product is crystallized from ethyl acetate to yield 5.38 gm (73%) of the title compound having a melting point of 195.3° C.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05011932
Quelldatensatzuspto-grants-1991_04
ORD IDord-074e7e8d13724821a24658b9785b6b98
Quellennotizuspto-grants-1991_04