HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-(Octyloxy)benzoic acid → 4-Octyloxybenzoyl chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-(Octyloxy)benzoic acid | HCID 17231 | — |
| Edukt | Phosphorus pentachloride | HCID 24819 | — |
| Lösungsmittel | Benzene | HCID 241 | — |
| Produkt | 4-Octyloxybenzoyl chloride | HCID 2760250 | — |
Reaktionsschritte
2.78 g of 4-octyloxybenzoic acid was added to 10 ml of benzene, and under stirring at room temperature, 2.36 g of PCl5 was added little by little. The mixture was then heated under reflux for 4 hours. Thereafter, the solvent was distilled off to obtain 4-octyloxybenzoic acid chloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05034152 |
| Quelldatensatz | uspto-grants-1991_07 |
| ORD ID | ord-d0c650b3ad4245688f41bd261bc78567 |
| Quellennotiz | uspto-grants-1991_07 |