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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1087407Erstellt: 25. Oktober 2026

Epichlorohydrin → 3-(1-Bromonaphth-2-yloxy)-1,2-epoxypropane

https://huagongshe.com/reaction/1087407

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktEpichlorohydrinHCID 7835—
Edukt1-Bromo-2-naphtholHCID 11316—
EduktPotassium CarbonateHCID 11430—
LösungsmittelMethyl Ethyl KetoneHCID 6569—
Produkt3-(1-Bromonaphth-2-yloxy)-1,2-epoxypropaneHCID 14369942—

Reaktionsschritte

A suspension containing 22.3 g of 1-bromonaphth-2-ol, 27.75 g of 1-chloro-2,3-epoxypropane and 27.6 g of potassium carbonate in 200 ml of butanone is refluxed overnight. The inorganic salts are filtered off and drained and the filtrate is then evaporated under vacuum. The oil obtained is distilled under 0.01 mm of mercury.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05036077
Quelldatensatzuspto-grants-1991_07
ORD IDord-e743b44489f04654891d9a3d50b33511
Quellennotizuspto-grants-1991_07