HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,3-Dibromopropane → 1,3-Bis(ortho-propenylphenoxy)propane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,3-Dibromopropane | HCID 8001 | — |
| Edukt | 2-Propenylphenol | HCID 93029 | — |
| Produkt | 1,3-Bis(ortho-propenylphenoxy)propane | HCID 54300370 | — |
Reaktionsschritte
1,3-bis(ortho-propenylphenoxy)propane is prepared in a procedure similar to Example I, except that 537 grams (4.0 moles) of propenyl phenol is employed along with 403 grams (1.98 moles) of 1,3-dibromo-propane to produce a reaction mixture extracted with methylene chloride and dried over magnesium sulfate, then vacuum distilled to give 311 grams (50% yield) of a solid with melting point 45°-48° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04962161 |
| Quelldatensatz | uspto-grants-1990_10 |
| ORD ID | ord-291fecb3e6064f8284170aa95bbf8f36 |
| Quellennotiz | uspto-grants-1990_10 |