HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1088427Erstellt: 27. Oktober 2026
m-Chloroperbenzoic acid → 4-(4,5-Epoxypentoxy)-4'-nitrobiphenyl
https://huagongshe.com/reaction/1088427
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | m-Chloroperbenzoic acid | HCID 70297 | — |
| Edukt | 4-(4-Pentenoxy)-4'-nitrobiphenyl | HCID 19901284 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | 4-(4,5-Epoxypentoxy)-4'-nitrobiphenyl | HCID 22163019 | — |
Reaktionsschritte
To 250 ml of methylene chloride is added 28.3 g of 4-(4-penteneoxy)-4'-nitrobiphenyl. The solution is cooled to 0° C., and 18 g of meta-chloroperbenzoic acid is added slowly. The mixture is stirred at 0° C. for 24 hours, and allowed to warm to room temperature.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US04962160 |
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| Quelldatensatz | uspto-grants-1990_10 |
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| ORD ID | ord-0ee21c4eba164910add49f0fd8393a22 |
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| Quellennotiz | uspto-grants-1990_10 |
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