N-Trimethylsilyl-N-methylacetamide → 1-Methyl-1-(N-methylacetamido)silacyclobutane

Beteiligte Stoffe

Reaktionsschritte

To 30.02 g 1-chloro-1-methylsilacyclobutane was added 36.10 g N-methyl-N-(trimethylsilyl)acetamide. The reaction products were fractionally distilled. The title compound was isolated as a clear, colorless fluid with a boiling point of 68°-76° C. at 3.6 mm Hg. The yield was 31.56 g (86%). The product was identified by NMR and mass spectroscopy.

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