Hydrochloric Acid → HCID 178432398, Verbindung

HRID 1089527Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1089527
[SH:1][C:2]1[N:7]2[N:8]=[C:9]([CH3:11])[N:10]=[C:6]2[N:5]=[C:4]([C:12]([O:14]C)=[O:13])[CH:3]=1.[OH-].[Na+].Cl>>[C:12]([C:4]1[CH:3]=[C:2]([SH:1])[N:7]2[N:8]=[C:9]([CH3:11])[N:10]=[C:6]2[N:5]=1)([OH:14])=[O:13]

Komponenten

4

Edukt 3

HCID 313Hydrochloric AcidHCID 14798Sodium HydroxideHCID 178498634HCID 178498634, Verbindung

Produkt 1

HCID 178432398HCID 178432398, VerbindungAusbeute 99,1 %

Versuchsvorschrift

A mixture of 7.7 g (34 mmole) of 7-mercapto-5-methoxycarbonyl-2-methyl-s-triazolo[1,5-a]pyrimidine and 70 ml of a 2N NaOH was stirred at room temperature for 2 hours and then ice-cooled. The pH of the mixture was adjusted to 2 with 6N HCl. The precipitates were collected by filtration and washed with water and then acetone, followed by drying, to obtain 7.08 g of the title compound (Yield: 99%).

Aufarbeitung

  1. temperatureice-cooled
  2. filtrationThe precipitates were collected by filtration
  3. washwashed with water
  4. customby drying

Quellen und Nachweise

ORD-Eintrag
ord-7c9374ae16a34cd0b0f16eedbcf77f02
Quelldatensatz
uspto-grants-1990_10
Patentnummer
US04966900

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